3LH0
Crystal structure of the 53BP1 tandem tudor domain in complex with p53K372me2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-01-11 |
Detector | NOIR-1 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 56.700, 78.280, 36.540 |
Unit cell angles | 90.00, 122.18, 90.00 |
Refinement procedure
Resolution | 30.927 - 1.900 |
R-factor | 0.222 |
Rwork | 0.221 |
R-free | 0.23210 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2g3r |
RMSD bond length | 0.033 |
RMSD bond angle | 1.896 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 2009_02_15_2320_3)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.927 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.049 | 0.188 |
Number of reflections | 10439 | |
<I/σ(I)> | 21.9 | 6.6 |
Completeness [%] | 97.6 | 95.8 |
Redundancy | 3.66 | 3.45 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.1 M HEPES-Na pH 7.0, 2% PEG 400 and 2.4 M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 298K |