3L9B
Crystal Structure of Rat Otoferlin C2A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-03-13 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | I 41 |
Unit cell lengths | 100.300, 100.300, 30.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.937 - 1.950 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dsy |
RMSD bond length | 0.006 |
RMSD bond angle | 0.981 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.1.4) |
Refinement software | PHENIX (1.5_2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.050 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.060 | 0.473 |
Number of reflections | 10992 | 1522 |
<I/σ(I)> | 15.03 | 2.6 |
Completeness [%] | 98.3 | 99.3 |
Redundancy | 3.01 | 2.93 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 277 | PEG 4000, MgCl2, pH 8.5, vapor diffusion, sitting drop, temperature 277K |