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3L82

X-ray Crystal structure of TRF1 and Fbx4 complex

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 21-ID-D
Synchrotron siteAPS
Beamline21-ID-D
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2008-03-23
DetectorMAR scanner 300 mm plate
Wavelength(s)0.9792, 0.9794
Spacegroup nameP 43 21 2
Unit cell lengths68.097, 68.097, 234.421
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.400
Rwork0.237
R-free0.26340
Structure solution methodMAD
RMSD bond length0.008
RMSD bond angle1.285
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSHARP
Refinement softwareCNS (1.1)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.400
Rmerge0.081
Number of reflections21197
<I/σ(I)>54.3
Completeness [%]96.2
Redundancy11.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION6.2289300 mM NH4H2PO4, 100 mM sodium citrate pH 6.2, 10% n-propanol and 10 mM DTT, VAPOR DIFFUSION, temperature 289K

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