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3L1Z

Crystal structure of the U-BOX domain of human E4B ubiquitin ligase in complex with UBCH5C E2 ubiquitin conjugating enzyme

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-BM
Synchrotron siteAPS
Beamline19-BM
Temperature [K]100
Detector technologyCCD
Collection date2006-02-10
DetectorADSC QUANTUM 210r
Wavelength(s)0.97918
Spacegroup nameP 6 2 2
Unit cell lengths142.708, 142.708, 83.133
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution32.780 - 3.170
R-factor0.2364
Rwork0.232
R-free0.27940
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)PDB ENTRIES 1L1X AND 3L1Y
RMSD bond length0.003
RMSD bond angle0.689
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]32.7803.230
High resolution limit [Å]3.1703.170
Rmerge0.1920.780
Number of reflections8196
<I/σ(I)>18.066.18
Completeness [%]92.296
Redundancy58.857.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP2954M sodium formate, VAPOR DIFFUSION, HANGING DROP, temperature 295K

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