3KX2
Crystal structure of Prp43p in complex with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-08-07 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.980 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 118.152, 118.152, 253.601 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.423 - 2.200 |
R-factor | 0.2085 |
Rwork | 0.206 |
R-free | 0.24970 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.013 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXS |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.300 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.012 | 0.750 |
Number of reflections | 104418 | |
Completeness [%] | 99.5 | 99.6 |
Redundancy | 4.2 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.75 | 277 | 100mM Mes-NaOH, pH 6.75, 14% PEG 8000, 300mM NaOAc, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.75 | 277 | 100mM Mes-NaOH, pH 6.75, 14% PEG 8000, 300mM NaOAc, VAPOR DIFFUSION, HANGING DROP, temperature 277K |