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3KQI

crystal structure of PHF2 PHD domain complexed with H3K4Me3 peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 22-ID
Synchrotron siteAPS
Beamline22-ID
Temperature [K]200
Detector technologyCCD
Collection date2009-07-31
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)1.0
Spacegroup nameP 65 2 2
Unit cell lengths77.757, 77.758, 72.116
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution7.990 - 1.780
R-factor0.1909
Rwork0.190
R-free0.21801
Structure solution methodSAD
RMSD bond length0.009
RMSD bond angle1.170
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSOLVE
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.840
High resolution limit [Å]1.7801.780
Rmerge0.0700.381
Number of reflections11858
<I/σ(I)>0.38963.83
Completeness [%]89.062.9
Redundancy94.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP62982.0 M ammonium sulfate, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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