3KMW
Crystal structure of the ILK/alpha-parvin core complex (MgATP)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-12-15 |
Detector | RIGAKU SATURN 944+ |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.134, 117.103, 47.393 |
Unit cell angles | 90.00, 101.96, 90.00 |
Refinement procedure
Resolution | 46.360 - 2.000 |
R-factor | 0.199 |
Rwork | 0.199 |
R-free | 0.20300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kmu |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.360 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 31165 | |
<I/σ(I)> | 12.2 | 7.8 |
Completeness [%] | 98.3 | 98.8 |
Redundancy | 5.53 | 6.09 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.8 | 277 | 0.05 M Bis-Tris, 12% PEG 5000 MME, 5% 1-propyl alcohol, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 277K |