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3KJ2

Mcl-1 in complex with Bim BH3 mutant F4aE

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2008-10-02
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameI 2 2 2
Unit cell lengths51.456, 71.487, 119.435
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution24.289 - 2.351
R-factor0.21
Rwork0.208
R-free0.24700
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.002
RMSD bond angle0.549
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Refinement softwarePHENIX
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.430
High resolution limit [Å]2.3505.0602.350
Rmerge0.0830.0400.449
Number of reflections9519
<I/σ(I)>9.2
Completeness [%]99.99999.8
Redundancy9.49.55.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP72980.1 M Imidazole, 0.2 M Zinc Acetate, 2% PEG 3350, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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