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3JVZ

E2~Ubiquitin-HECT

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Detector technologyCCD
Collection date2008-07-31
DetectorADSC QUANTUM 315
Spacegroup nameC 2 2 21
Unit cell lengths173.980, 199.888, 109.707
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 3.300
R-factor0.217
Rwork0.217
R-free0.26700
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2C4O.pdb 2ONI.pdb
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0003.420
High resolution limit [Å]3.3003.300
Rmerge0.0920.568
Number of reflections25449
<I/σ(I)>14.552.37
Completeness [%]89.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.12770.1 M sodium citrate, pH 5.1-5.2, 2.4-2.5 M sodium chloride, VAPOR DIFFUSION, HANGING DROP, temperature 277K

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