3JVF

Crystal structure of an Interleukin-17 receptor complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-2
Synchrotron site	SSRL
Beamline	BL9-2
Temperature [K]	100
Collection date	2008-04-16
Wavelength(s)	1.00
Spacegroup name	P 41 21 2
Unit cell lengths	170.730, 170.730, 81.900
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.821 - 3.300
R-factor	0.2305
Rwork	0.229
R-free	0.25570
Structure solution method	SIRAS
RMSD bond length	0.009
RMSD bond angle	1.333
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	SHARP
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
High resolution limit [Å]	3.300
Number of reflections	18749

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9.2	295	PEG6000, 0.1M CAPSO, calcium chloride, pH 9.2, VAPOR DIFFUSION, HANGING DROP, temperature 295K
1	VAPOR DIFFUSION, HANGING DROP	9.2	295	PEG6000, 0.1M CAPSO, calcium chloride, pH 9.2, VAPOR DIFFUSION, HANGING DROP, temperature 295K
1	VAPOR DIFFUSION, HANGING DROP	9.2	295	PEG6000, 0.1M CAPSO, calcium chloride, pH 9.2, VAPOR DIFFUSION, HANGING DROP, temperature 295K
1	VAPOR DIFFUSION, HANGING DROP	9.2	295	PEG6000, 0.1M CAPSO, calcium chloride, pH 9.2, VAPOR DIFFUSION, HANGING DROP, temperature 295K