3IPY
X-Ray structure of Human Deoxycytidine Kinase in complex with an inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 4.2.2 |
| Synchrotron site | ALS |
| Beamline | 4.2.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-05-07 |
| Detector | NOIR-1 |
| Wavelength(s) | 1.00 |
| Spacegroup name | I 21 21 21 |
| Unit cell lengths | 74.556, 74.428, 239.097 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 119.520 - 2.540 |
| R-factor | 0.2168 |
| Rwork | 0.214 |
| R-free | 0.27313 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1p60 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.404 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 119.520 |
| High resolution limit [Å] | 2.540 |
| Number of reflections | 20090 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.1 M sodium acetate, 25% PEG 4000, 8% isopropanol |
