3I7I
MMP-13 in complex with a non zinc-chelating inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 134.186, 35.777, 95.295 |
Unit cell angles | 90.00, 131.08, 90.00 |
Refinement procedure
Resolution | 30.862 - 2.208 |
R-factor | 0.235 |
Rwork | 0.230 |
R-free | 0.31400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.993 |
Refinement software | PHENIX (1.4_6) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 66.960 |
High resolution limit [Å] | 2.208 |
Number of reflections | 17300 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |