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3HV7

Human p38 MAP Kinase in Complex with RL38

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsBRUKER AXS MICROSTAR
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2008-05-06
DetectorMAR scanner 300 mm plate
Wavelength(s)1.54170
Spacegroup nameP 21 21 21
Unit cell lengths66.710, 74.520, 78.910
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution34.870 - 2.400
R-factor0.208
Rwork0.203
R-free0.27900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1zyj
RMSD bond length0.016
RMSD bond angle1.620
Data reduction softwareMOSFLM
Data scaling softwareXSCALE
Phasing softwarePHASER (1.3.1)
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.0002.530
High resolution limit [Å]2.4002.400
Rmerge0.0690.357
Number of reflections159273910
<I/σ(I)>17.15.2
Completeness [%]99.9100
Redundancy4.84.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP5.8293100 mM MES, 20-30% PEG4000, 50 mM n-BOG, pH 5.8, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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