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3HTM

Structures of SPOP-Substrate Complexes: Insights into Molecular Architectures of BTB-Cul3 Ubiquitin Ligases: SPOPBTB/3-box

Experimental procedure
Experimental methodSAD
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X25
Synchrotron siteNSLS
BeamlineX25
Collection date2005-04-20
Spacegroup nameP 1
Unit cell lengths36.800, 88.700, 88.700
Unit cell angles90.80, 89.30, 89.90
Refinement procedure
Resolution44.340 - 2.500
R-factor0.217
Rwork0.217
R-free0.25600
Structure solution methodSAD
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSOLVE
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.510
High resolution limit [Å]2.4202.420
Number of reflections37547
<I/σ(I)>25.54.9
Redundancy1.91.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROPVAPOR DIFFUSION, HANGING DROP

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PDB entries from 2024-11-06

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