3HMW
Crystal structure of ustekinumab FAB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-007 HF |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-02-18 |
| Detector | RIGAKU SATURN 944 |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 139.310, 139.310, 114.580 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.827 - 3.000 |
| R-factor | 0.231 |
| Rwork | 0.228 |
| R-free | 0.28700 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.757 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | CNX |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 69.650 | 3.110 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.107 | 0.361 |
| Number of reflections | 13596 | |
| <I/σ(I)> | 25.5 | 9 |
| Completeness [%] | 99.6 | 98.7 |
| Redundancy | 40 | 38.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
