3HMJ
Saccharomyces cerevisiae FAS type I
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 100 |
| Wavelength(s) | 1.039 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 231.884, 231.884, 756.784 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.999 - 4.000 |
| R-factor | 0.2662 |
| Rwork | 0.266 |
| R-free | 0.26720 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2vkz |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.167 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 4.300 |
| High resolution limit [Å] | 4.000 | 4.000 |
| Number of reflections | 168120 | |
| Completeness [%] | 97.0 | 97 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | PEG, pH7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
