3HA8
THE COMPLEX STRUCTURE OF THE MAP KINASE P38/Compound 14b
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Collection date | 2008-02-15 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 46.222, 87.934, 121.501 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 25.000 - 2.480 |
| R-factor | 0.21685 |
| Rwork | 0.215 |
| R-free | 0.24780 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1bmk |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.069 |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.480 |
| Number of reflections | 17710 |
| Completeness [%] | 97.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
