3H9O
Phosphoinositide-dependent protein kinase 1 (PDK-1) in complex with compound 9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 93 |
Detector technology | CCD |
Detector | BRUKER SMART 6000 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 123.770, 123.770, 47.116 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.469 - 2.300 |
R-factor | 0.2112 |
Rwork | 0.209 |
R-free | 0.25580 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | SAINT |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 107.200 |
High resolution limit [Å] | 2.300 |
Number of reflections | 18783 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP |