3GVR
Single-chain UROD Y164G (GY) mutation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-08-18 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 103.447, 103.447, 70.716 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 14.730 - 2.200 |
R-factor | 0.197 |
Rwork | 0.194 |
R-free | 0.24600 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.243 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 2.280 |
High resolution limit [Å] | 2.200 | 4.740 | 2.200 |
Rmerge | 0.110 | 0.069 | 0.395 |
Number of reflections | 22288 | ||
<I/σ(I)> | 15.353 | ||
Completeness [%] | 99.3 | 96.1 | 98.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | hanging drop |