3GVQ
UROD single-chain dimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-09-11 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 103.145, 103.145, 71.287 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 30.000 - 2.100 |
R-factor | 0.19517 |
Rwork | 0.193 |
R-free | 0.24411 |
Structure solution method | MR |
Starting model (for MR) | 1uro |
RMSD bond length | 0.013 |
RMSD bond angle | 1.265 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.070 | 0.400 |
Number of reflections | 25394 | |
<I/σ(I)> | 9.9 | 2.2 |
Completeness [%] | 98.0 | 86.3 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 298 | CITRATE BUFFER, PH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 298K |