Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 116.700, 104.300, 48.490 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.200 |
R-factor | 0.141 |
RMSD bond length | 0.014 |
RMSD bond angle | 0.029 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.100 * |
Rmerge | 0.044 * |
Total number of observations | 233315 * |
Number of reflections | 33871 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 5.95 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 15 (mg/ml) | |
2 | 1 | drop | potassium phosphate | 50 (mM) | |
3 | 1 | drop | PEG6000 | 13 (%(w/v)) | |
4 | 1 | reservoir | phosphate | 50 (mM) | |
5 | 1 | reservoir | PEG6000 | 30 (%(w/v)) |