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3GL6

Crystal structure of JARID1A-PHD3 complexed with H3(1-9)K4me3 peptide

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Temperature [K]197
Detector technologyCCD
Collection date2008-07-05
DetectorADSC QUANTUM 315
Wavelength(s)0.97949
Spacegroup nameI 41
Unit cell lengths49.950, 49.950, 86.450
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 1.900
R-factor0.222
Rwork0.208
R-free0.22500
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.006
RMSD bond angle1.430
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASES
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.970
High resolution limit [Å]1.9001.900
Number of reflections8172
<I/σ(I)>55.56.46
Completeness [%]97.685.1
Redundancy84.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52930.1M Hepes-Na, 10% iso-propanol, 20% PEG4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K
1VAPOR DIFFUSION, HANGING DROP7.52930.1M Hepes-Na, 10% iso-propanol, 20% PEG4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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