3GEQ
Structural basis for the chemical rescue of Src kinase activity
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-02-15 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 59.649, 63.462, 83.860 |
格子定数 [度] | 90.00, 91.45, 90.00 |
精密化法
残基 | 50.000 - 2.200 |
Rwork | 0.226 |
R-free | 0.27300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2src |
結合長の平均二乗偏差(RMSD) [Å] | 0.074 |
結合角の平均二乗偏差(RMSD) [度] | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASES |
Refinement software | CNS |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.280 |
分解能 [Å] (高) | 2.200 | 2.200 |
独立反射数 | 31912 | |
完全性 [%] | 98.7 | 93.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 50 mM Ammoniumacetate, 100 mM Bis-Tris pH 5.5, 1 mM DTT, 50 mM imidazole, 0.5 mM PP2, VAPOR DIFFUSION, HANGING DROP, temperature 298K |