3GCW
PCSK9:EGFA(H306Y)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Detector technology | CCD |
Collection date | 2008-08-09 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 115.661, 115.661, 133.401 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.100 - 2.700 |
R-factor | 0.23624 |
Rwork | 0.234 |
R-free | 0.27780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3bps |
RMSD bond length | 0.006 |
RMSD bond angle | 0.971 |
Refinement software | REFMAC (5.3.0037) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.770 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.081 | |
Number of reflections | 25367 | |
Completeness [%] | 99.3 | 92.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 294 | 0.3M (NH4)H2PO4, pH 7.4, VAPOR DIFFUSION, SITTING DROP, temperature 294K |