3FZJ
TsaR low resolution crystal structure, tetragonal form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-06-27 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9326 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 204.370, 204.370, 336.210 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.340 - 7.100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fxq |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.570 | 7.100 |
High resolution limit [Å] | 7.000 | 7.000 |
Rmerge | 0.109 | 0.662 |
Number of reflections | 11779 | |
<I/σ(I)> | 17.09 | 2.74 |
Completeness [%] | 99.3 | 100 |
Redundancy | 7.73 | 8.15 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 298 | 2M Ammonium phosphate, 0.1M Tris-HCl, pH 8.5, microbatch under oil, temperature 298K |