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3FJE

Crystal structure of C83S mutant of Human acidic fibroblast growth factor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH2R
Temperature [K]103
Detector technologyIMAGE PLATE
Collection date2005-11-14
DetectorRIGAKU RAXIS IIC
Wavelength(s)1.5418
Spacegroup nameC 2 2 21
Unit cell lengths75.414, 94.393, 108.654
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution28.730 - 2.100
R-factor0.198
Rwork0.198
R-free0.23500
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1jqz
RMSD bond length0.008
RMSD bond angle1.400
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]28.7302.150
High resolution limit [Å]2.1002.100
Rmerge0.0770.248
Number of reflections21360
<I/σ(I)>6.78
Completeness [%]92.9100
Redundancy10.110
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.52983.0M Na formate, 0.4M (NH4)2SO4, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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