3FIG
Crystal Structure of Leucine-bound LeuA from Mycobacterium tuberculosis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.207, 154.258, 68.669 |
Unit cell angles | 90.00, 97.99, 90.00 |
Refinement procedure
Resolution | 27.660 - 2.300 |
R-factor | 0.17 |
Rwork | 0.166 |
R-free | 0.24400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1sr9 |
RMSD bond length | 0.024 |
RMSD bond angle | 2.029 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.300 |
Number of reflections | 49393 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 291 | Sodium Citrate, MPEG 2000, pH 6.0, Vapor diffusion, sitting drop, temperature 291K |