Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2008-05-05 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.97935 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 55.590, 55.489, 324.101 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.790 - 2.100 |
| R-factor | 0.203 |
| Rwork | 0.199 |
| R-free | 0.26800 |
| RMSD bond length | 0.026 |
| RMSD bond angle | 2.185 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 2.130 |
| High resolution limit [Å] | 2.060 | 4.440 | 2.060 |
| Rmerge | 0.068 | 0.041 | 0.723 |
| Number of reflections | 54977 | ||
| <I/σ(I)> | 24.9 | ||
| Completeness [%] | 86.9 | 99.2 | 62.4 |
| Redundancy | 5.4 | 6.1 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.6 | 300 | 10% PEG 4000, 0.1M Sodium Citrate, pH 5.6, VAPOR DIFFUSION, HANGING DROP, temperature 300K |
