3EXS
Crystal structure of KGPDC from Streptococcus mutans in complex with D-R5P
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | OTHER |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-05-21 |
Detector | BRUKER SMART 6000 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.152, 124.249, 130.066 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.740 - 2.500 |
R-factor | 0.18661 |
Rwork | 0.184 |
R-free | 0.24386 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ext |
RMSD bond length | 0.013 |
RMSD bond angle | 1.367 |
Data scaling software | SAINT |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.740 |
High resolution limit [Å] | 2.500 |
Number of reflections | 31798 |
Completeness [%] | 93.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 0.2M KCl, 0.05M HEPES, pH7.5, 35%(v/v) pentaerythritol propoxylate (5/4 PO/OH), VAPOR DIFFUSION, HANGING DROP, temperature 289K |