3EWD

Crystal structure of adenosine deaminase mutant (delta Asp172) from Plasmodium vivax in complex with MT-coformycin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X29A
Synchrotron site	NSLS
Beamline	X29A
Temperature [K]	100
Detector technology	CCD
Collection date	2008-10-02
Detector	ADSC QUANTUM 315
Wavelength(s)	0.97910
Spacegroup name	P 21 21 21
Unit cell lengths	41.905, 86.975, 106.103
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 1.900
R-factor	0.20346
Rwork	0.201
R-free	0.24961
RMSD bond length	0.018
RMSD bond angle	1.767
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.4.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.930
High resolution limit [Å]	1.900	1.900
Rmerge	0.097	0.675
Number of reflections	31244
<I/σ(I)>	14.753	2.36
Completeness [%]	99.9	100
Redundancy	5.5	5.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1