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3ETM

Crystal structure of the mimivirus NDK +KPN-N62L-R107G triple mutant complexed with CDP

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSEALED TUBE
Source detailsOXFORD DIFFRACTION ENHANCE ULTRA
Temperature [K]105
Detector technologyCCD
Collection date2007-09-27
DetectorOXFORD ONYX CCD
Wavelength(s)1.54
Spacegroup nameP 63
Unit cell lengths70.325, 70.325, 104.279
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution29.231 - 1.900
R-factor0.176
Rwork0.173
R-free0.21800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2b8p
RMSD bond length0.008
RMSD bond angle1.350
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareAMoRE
Refinement softwarePHENIX
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.4002.000
High resolution limit [Å]1.9001.900
Number of reflections22776
<I/σ(I)>6.92.2
Completeness [%]98.994.5
Redundancy3.11.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.62930.8 to 1M sodium citrate, 0.1M Tris, pH 7.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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