3ENA
Crystal structure of the mimivirus NDK +Kpn-N62L-R107G triple mutant complexed with dGDP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2007-09-09 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.934 |
Spacegroup name | P 63 |
Unit cell lengths | 70.358, 70.358, 104.295 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 52.611 - 1.600 |
R-factor | 0.17 |
Rwork | 0.168 |
R-free | 0.20200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b8p |
RMSD bond length | 0.007 |
RMSD bond angle | 1.191 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.600 | 1.690 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.042 | 0.229 |
Number of reflections | 38444 | |
<I/σ(I)> | 11.2 | 3.3 |
Completeness [%] | 99.8 | |
Redundancy | 5 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.6 | 293 | 0.8 to 1.1M sodium citrate, 0.1M tris, pH 7.6, VAPOR DIFFUSION, HANGING DROP, temperature 293K |