3E7Z

Structure of human insulin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	BRUKER AXS MICROSTAR
Temperature [K]	100
Detector technology	CCD
Detector	BRUKER SMART 6000
Spacegroup name	H 3
Unit cell lengths	82.741, 82.741, 34.060
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	8.000 - 1.700
R-factor	0.2
Rwork	0.196
R-free	0.27120
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3e7y
RMSD bond length	0.006
RMSD bond angle	0.966
Refinement software	PHENIX ((phenix.refine))

Data quality characteristics

	Overall
Low resolution limit [Å]	9.800
High resolution limit [Å]	1.700
Number of reflections	9103

Crystallization Conditions

crystal ID	method	pH	temperature	details
1