3E7F
Crystal structure of 6-phosphogluconolactonase from Trypanosoma brucei complexed with 6-phosphogluconic acid
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-3 |
| Synchrotron site | ESRF |
| Beamline | ID14-3 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2006-10-01 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.931 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.660, 87.000, 64.910 |
| Unit cell angles | 90.00, 96.43, 90.00 |
Refinement procedure
| Resolution | 23.960 - 2.200 |
| R-factor | 0.1776 |
| Rwork | 0.174 |
| R-free | 0.24930 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.302 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | MOLREP |
| Refinement software | BUSTER-TNT (2.1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.000 | 2.500 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Number of reflections | 27717 | |
| Completeness [%] | 99.3 | 86.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
