3E6A
Crystal structure and Functional Analysis of Glyceraldehyde-3-phosphate Dehydrogenase from Oryza Sativa
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL12B2 |
| Synchrotron site | SPring-8 |
| Beamline | BL12B2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-06-17 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 76.258, 127.418, 77.385 |
| Unit cell angles | 90.00, 118.05, 90.00 |
Refinement procedure
| Resolution | 30.000 - 3.770 |
| Rwork | 0.196 |
| R-free | 0.21000 |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 3.770 |
| Number of reflections | 16104 |
| Completeness [%] | 99.1 |
| Redundancy | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.1 | 293 | 0.05M Ammonium sulfate, 0.05M Bis-Tris, 40% (w/v) 15/4 EO/OH, pH 6.1, vapor diffusion, hanging drop, temperature 293K |
