3DZJ

Crystal structure of human CD38 extracellular domain E226Q mutant, NMN complex

Refinement Statistics

Experimental method:X-RAY DIFFRACTION (1.9 Å)

Cell axes41.85853.22865.670
Cell angles106.1191.9795.03
SpacegroupP 1
Resolution limits20.00 - 1.90
the highest resolution shell value1.950 - 1.900
R-factor0.188
R-work0.18500
the highest resolution shell value0.233
R-free0.24100
the highest resolution shell value0.299
RMSD bond length0.019
RMSD bond angle1.772

Data Collection Statistics

Resolution limits30.00 - 1.90
the highest resolution shell value -
Number of reflections41633
Rmerge_l_obs0.090
the highest resolution shell value0.436
Completeness97.5
Redundancy3.8
the highest resolution shell value2.9
I/sigma(I)3

Crystallization Conditions

crystal IDmethodpHpH rangetemperatureunit
16298

Crystallization Reagents

IDcrystal IDsolution IDreagent nameconcentrationdetails
Crystallization Reagents in Literatures*
IDcrystal IDsolutionreagent nameconcentration (unit)details
Annotated Information is extracted from Literature Info*