3DYN
human phosphodiestrase 9 in complex with cGMP (Zn inhibited)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Detector technology | CCD |
Collection date | 2006-07-26 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 103.857, 103.857, 270.118 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.100 |
R-factor | 0.18251 |
Rwork | 0.180 |
R-free | 0.20274 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 1TBM |
RMSD bond length | 0.013 |
RMSD bond angle | 1.120 |
Refinement software | REFMAC (5.3.0008) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.100 |
Rmerge | 0.090 |
Number of reflections | 77963 |
<I/σ(I)> | 18.1 |
Completeness [%] | 99.8 |
Redundancy | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |