3DXE
Crystal structure of the intracellular domain of human APP (T668A mutant) in complex with Fe65-PTB2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-07-19 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.975 |
Spacegroup name | P 61 |
Unit cell lengths | 115.377, 115.377, 75.523 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.320 - 2.000 |
R-factor | 0.208 |
Rwork | 0.206 |
R-free | 0.24100 |
RMSD bond length | 0.019 |
RMSD bond angle | 1.569 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SOLVE |
Refinement software | REFMAC (5.3.0008) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.000 | 2.110 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.119 | 0.612 |
Number of reflections | 37351 | |
<I/σ(I)> | 23.1 | 3.1 |
Completeness [%] | 97.9 | 95.3 |
Redundancy | 15 | 15.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.6 | 293 | 3.2 M NaCl, 0.1 M sodium acetate , pH 4.6, VAPOR DIFFUSION, temperature 293K |