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3DUH

Structure of Interleukin-23

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL11-1
Synchrotron siteSSRL
BeamlineBL11-1
Temperature [K]140
Detector technologyCCD
Collection date2008-05-04
DetectorMARMOSAIC 325 mm CCD
Wavelength(s)1.0
Spacegroup nameC 1 2 1
Unit cell lengths116.089, 59.974, 160.365
Unit cell angles90.00, 90.46, 90.00
Refinement procedure
Resolution30.000 - 2.300
R-factor0.23007
Rwork0.228
R-free0.26833
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)human p40 from PDB ID 1F45
RMSD bond length0.012
RMSD bond angle1.527
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.420
High resolution limit [Å]2.3002.300
Rmerge0.0730.556
Number of reflections49424
<I/σ(I)>13.62.5
Completeness [%]99.9100
Redundancy3.73.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP729520% PEG3350, 0.2M potassium nitrate, 0.1M Hepes-NaOH pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 295K

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