3DLS
Crystal structure of human PAS kinase bound to ADP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 31-ID |
| Synchrotron site | APS |
| Beamline | 31-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2008-04-22 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.97929 |
| Spacegroup name | P 1 |
| Unit cell lengths | 85.778, 85.840, 94.154 |
| Unit cell angles | 77.28, 77.50, 60.09 |
Refinement procedure
| Resolution | ? - 2.300 |
| R-factor | 0.244 |
| Rwork | 0.241 |
| R-free | 0.29700 |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 96809 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 293 | 10% GLYCEROL, 18% PEG 3350, 150 mM CALCIUM ACETATE, pH 7.5, VAPOR DIFFUSION, temperature 293K |
