3DBN
Crystal structure of the Streptoccocus suis serotype2 D-mannonate dehydratase in complex with its substrate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 105.520, 105.520, 160.077 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.900 |
R-factor | 0.23373 |
Rwork | 0.231 |
R-free | 0.28031 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.579 |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 88.040 |
High resolution limit [Å] | 2.900 |
Number of reflections | 20245 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |