3D7B
The Ribonuclease A- 5'-Deoxy-5'-N-pyrrolidinouridine complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE PX9.6 |
Synchrotron site | SRS |
Beamline | PX9.6 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-11-07 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.92 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 99.959, 32.540, 72.439 |
Unit cell angles | 90.00, 90.62, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.600 |
R-factor | 0.18041 |
Rwork | 0.179 |
R-free | 0.21330 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | : 2G8Q |
RMSD bond length | 0.007 |
RMSD bond angle | 1.429 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | REFMAC |
Refinement software | REFMAC (5.3.0037) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 30196 | |
<I/σ(I)> | 11.7 | 3 |
Completeness [%] | 96.4 | 95.9 |
Redundancy | 3.2 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | PEG 4000, SODIUM CITRATE, pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |