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3D59

Crystal structure of human plasma platelet activating factor acetylhydrolase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2006-03-17
DetectorADSC QUANTUM 315
Wavelength(s)1.100
Spacegroup nameC 1 2 1
Unit cell lengths116.184, 83.061, 96.705
Unit cell angles90.00, 115.09, 90.00
Refinement procedure
Resolution10.000 - 1.500
R-factor0.131
Rwork0.131
R-free0.19100
Structure solution methodMAD
RMSD bond length0.011
RMSD bond angle0.027
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareSOLVE
Refinement softwareSHELXL-97
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.550
High resolution limit [Å]1.5001.500
Rmerge0.0570.283
Number of reflections127359
<I/σ(I)>19.191.92
Completeness [%]96.475.7
Redundancy3.61.8
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
16.6293PH 6.6, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K, pH 6.60
16.6293PH 6.6, VAPOR DIFFUSION, HANGING DROP, temperature 293.0K, pH 6.60

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