Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-09-06 |
| Wavelength(s) | 1.0083 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 41.715, 74.172, 55.516 |
| Unit cell angles | 90.00, 94.67, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.510 |
| Rwork | 0.206 |
| R-free | 0.22900 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | CNS |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 1.560 |
| High resolution limit [Å] | 1.510 | 3.250 | 1.510 |
| Rmerge | 0.112 | 0.037 | 0.724 |
| Number of reflections | 48197 | ||
| <I/σ(I)> | 6.2 | ||
| Completeness [%] | 91.0 | 99.9 | 47.5 |
| Redundancy | 6.4 | 7.4 | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.4 | 292 | 0.1M cacodylate, 25% PEG5000MME, 0.2M ammonium sulfate, pH 7.4, VAPOR DIFFUSION, temperature 292K |
