3CMJ
Crystal Structure of engineered Beta-Glucosidase from Soil metagenome
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 6C1 |
Synchrotron site | PAL/PLS |
Beamline | 6C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-08 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.23986 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.331, 71.002, 86.978 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.600 |
R-factor | 0.165 |
Rwork | 0.163 |
R-free | 0.19800 |
Starting model (for MR) | PDB code 1OIM |
RMSD bond length | 0.010 |
RMSD bond angle | 1.341 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASES |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.660 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 54735 | |
<I/σ(I)> | 35.57 | |
Completeness [%] | 94.0 | |
Redundancy | 5 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 295 | Na/K tartrate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |