3CH3
Crystal Structure Analysis of SERA5E from plasmodium falciparum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-ID-B |
Synchrotron site | APS |
Beamline | 14-ID-B |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.968 |
Spacegroup name | H 3 |
Unit cell lengths | 103.368, 103.368, 72.508 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.740 - 1.790 |
R-factor | 0.1693 |
Rwork | 0.168 |
R-free | 0.19844 |
Structure solution method | SAD |
RMSD bond length | 0.014 |
RMSD bond angle | 1.361 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 24.740 |
High resolution limit [Å] | 1.790 |
Number of reflections | 26819 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | 0.2M KH2PO4, 12% PEG 8000, 5% PEG 400, pH 4.6, VAPOR DIFFUSION, SITTING DROP, temperature 298K |