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3CGU

Crystal Structure of unliganded Argos

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Temperature [K]100
Detector technologyCCD
Collection date2005-11-09
DetectorADSC QUANTUM 315r
Spacegroup nameC 1 2 1
Unit cell lengths113.583, 64.246, 72.530
Unit cell angles90.00, 101.59, 90.00
Refinement procedure
Resolution35.530 - 2.510
R-factor0.258
Rwork0.256
R-free0.29900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3c9a
RMSD bond length0.009
RMSD bond angle1.029
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.580
High resolution limit [Å]2.5102.510
Rmerge0.0550.364
Number of reflections15720
<I/σ(I)>15.12.7
Completeness [%]93.980.9
Redundancy3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
14.529110-20% PEG3350, 0.1M NaAcetate pH 4.5, 0.2M ammonium sulphate, VAPOR DIFFUSION, HANGING DROP, temperature 291K, pH 4.50

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