Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL11-1 |
| Synchrotron site | SSRL |
| Beamline | BL11-1 |
| Temperature [K] | 177 |
| Detector technology | CCD |
| Collection date | 2004-08-01 |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | P 3 |
| Unit cell lengths | 144.900, 144.900, 164.400 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 23.000 - 3.500 |
| R-factor | 0.271 |
| Rwork | 0.271 |
| R-free | 0.28500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.330 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 23.000 |
| High resolution limit [Å] | 3.100 |
| Rmerge | 0.117 |
| Number of reflections | 60820 |
| <I/σ(I)> | 8.8 |
| Completeness [%] | 85.0 |
| Redundancy | 4.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298 | AMMONIUM FLUORIDE, CITRATE BUFFER, SODIUM DIHYDROGEN PHOSPHATE, PEG 400, pH 5.00, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
