3C8E
Crystal Structure Analysis of yghU from E. Coli
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-06-22 |
Detector | MAR |
Wavelength(s) | 1.00, 0.9795, 0.9790, 0.9500 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.197, 73.455, 130.810 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.500 |
R-factor | 0.165 |
Rwork | 0.162 |
R-free | 0.19700 |
Structure solution method | MAD |
RMSD bond length | 0.019 |
RMSD bond angle | 1.834 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELX |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.460 |
High resolution limit [Å] | 1.410 | 3.040 | 1.410 |
Rmerge | 0.109 | 0.055 | 0.653 |
Number of reflections | 95609 | ||
<I/σ(I)> | 7.1 | ||
Completeness [%] | 87.7 | 99.6 | 56.5 |
Redundancy | 8.7 | 13.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 298 | 0.1M Bis-Tris pH 5.5, 0.2M NaCl, 25% w/v PEG 3350, VAPOR DIFFUSION, HANGING DROP, temperature 298K |