3C5K
Crystal structure of human HDAC6 zinc finger domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X29A |
Synchrotron site | NSLS |
Beamline | X29A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-01-26 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.26000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.500, 45.109, 55.759 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.070 - 1.550 |
R-factor | 0.1759 |
Rwork | 0.173 |
R-free | 0.22663 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.151 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SOLVE |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.610 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.071 | 0.201 |
Number of reflections | 15138 | |
<I/σ(I)> | 13.3 | 5.84 |
Completeness [%] | 98.0 | 80.5 |
Redundancy | 10.8 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 297 | 3.5M Na formate, 100mM Bis-tris propane pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 297K |